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Abstract The growth and decay of the Laurentide ice sheet altered the hydrological cycle over southwestern North America. While it is well‐documented that the last glacial was wetter and had isotopically lighter precipitation, much less information is available for prior glacials. Increased proxy coverage is needed to test climate models' ability to reconstruct these changes and to assess their predictive power for water availability in response to future climate change. Here, we present parallel precipitation isotope records spanning the last two glacial cycles from two large, proximal lakes in Utah, USA: Great Salt Lake and Bear Lake. We use plant waxn‐alkane δD as a proxy for precipitation δD (δD_precip) and find coherent glacial‐interglacial fluctuations in δD_precip, with a ∼30‰ D‐depletion during glacial maxima relative to interglacials. We find similar δD_precipvalues between the Holocene and Eemian, but at the lower‐pCO₂MIS 7 interglacial, D‐enrichment is only weakly recorded at Great Salt Lake and absent at higher elevation Bear Lake. Comparison to regional proxy archives finds large‐scale coherence in regional hydroclimate change over the last two glacial cycles is best explained by thermodynamic processes, with increased rainout efficiency, isotopic fractionation, and snow in a colder atmosphere. Comparison of proxies to climate model experiments showed models considerably underestimate glacial lowering of precipitation isotopic values, but overestimate inland Rayleigh distillation. New and assembled proxy reconstructions provide greater temporal and spatial coverage as targets for model skill in capturing hydroclimate variations across the past two glacial cycles. 

Abstract Great Salt Lake, Utah, is a hypersaline terminal lake in the Great Basin, and the remnant of the late glacial Lake Bonneville. Holocene hydroclimate variations cannot be interpreted from the shoreline record, but instead can be investigated by proxies archived in the sediments. GLAD1-GSL00-1B was cored in 2000 and recently dated by radiocarbon for the Holocene section with the top 11 m representing ∼7 ka to present. Sediment samples every 30 cm (∼220 years) were studied for the full suite of microbial membrane lipids, including those responsive to temperature and salinity. The Archaeol and Caldarchaeol Ecometric (ACE) index detects the increase in lipids of halophilic archaea, relative to generalists, as salinity increases. We find Holocene ACE values ranged from 81-98, which suggests persistent hypersalinity with <50 g/L variability across 7.2 ka. The temperature proxy, MBTʹ5Me, yields values similar to modern mean annual air temperature for months above freezing (MAF = 15.7°C) over the last 5.5 ka. Several GDGT metrics show a step shift in microbial communities and limnology at 5.5 ka. Extended archaeol detects elevated salinity during the regional mid-Holocene drought, not readily detected in the ACE record that is often near the upper limit of the index. We infer that the mid-Holocene GSL was shallower and saltier than the late Holocene. The current drying may be returning the lake to conditions not seen since the mid-Holocene. Plain Language Summary Great Salt Lake in Utah is the remnant of a once much larger lake and is currently at a historically low level. We study a lake sediment core, collected in 2000 from the floor of Great Salt Lake, and recently dated. We take new samples from the core and measure them for molecules made by microbes, whether living in the lake or washed in from the surrounding soils. We reconstruct lake conditions during the last 7,200 years and assess whether lake level fluctuated during that time. Over the past 7,200 years, we find evidence that the lake was shallower from 7,200 to 5,500 years ago but has been relatively stable until the modifications of the lake in the 20th century and the current drying trend. 

Abstract Carbonate minerals are a major reservoir in the global carbon cycle and a key player in the sequestration and emission of atmospheric CO 2 . In addition to the minerals’ frequent use in agriculture and construction, carbonate formation has been targeted for anthropogenic CO 2 sequestration. Due to carbonate’s importance in geological and anthropogenic realms, research on carbonate characterization and quantification is of interest. Here, we demonstrate a method to identify and quantify calcite (CaCO 3 ) and dolomite (CaMg(CO 3 ) 2 ) in sediment matrices using diffuse reflectance infrared Fourier transform spectroscopy (DRIFTS). Needing only a few minutes per sample, DRIFTS is a rapid technique that does not require hazardous chemicals and does not destroy samples during analysis. We selected the 2515 ± 9 cm −1 absorbance bands for quantification as they exhibited little interference from sediment matrix minerals and large peak areas relative to other bands. The DRIFTS technique was compared to the traditional acidification headspace analysis method on artificial mixtures of sediment and carbonate as well as natural lake bed and river bank samples from the Upper Sangamon River Basin in Illinois, USA. DRIFTS offers an additional advantage over acidification in that it permits carbonate mineral identification simultaneously with its quantification. Though DRIFTS estimates were higher, a good correlation was found between DRIFTS and acidification estimates for both lake sediments ( R 2  = 0.99) and bank samples ( R 2  = 0.92), indicating DRIFTS is a reliable method for carbonate quantification in sediment matrices.